Porosity and Micro-Hardness of Shrouded Plasma Sprayed Titanium Coatings

Titanium and its alloys are often used as key materials for corrosion protection. A promising approach to optimize both mechanical properties and corrosion resistance is the use of coating technologies. In this paper, shrouded plasma spray was used as a useful technology to produce low oxide containing titanium coatings. A solid shroud was used to plasma spray titanium coatings to reduce the oxide content. The titanium coatings were assessed by optical microscope, scanning electron microscopy and Vickers microhardness testing. The results showed that the shrouded titanium coatings exhibited an enhanced microstructure. The presence of the shroud and shroud gas flow led to a significant reduction in coating porosity because the reduction in air entrainment with the shroud resulted in better heating of the particles. The shrouded titanium coatings had a lower value of Vickers microhardness and a relative lower standard deviation than the air plasma sprayed titanium coatings

Porosity and Micro-Hardness of Shrouded Plasma Sprayed Titanium Coatings

Titanium and its alloys are often used as key materials for corrosion protection. A promising approach to optimize both mechanical properties and corrosion resistance is the use of coating technologies. In this paper, shrouded plasma spray was used as a useful technology to produce low oxide containing titanium coatings. A solid shroud was used to plasma spray titanium coatings to reduce the oxide content. The titanium coatings were assessed by optical microscope, scanning electron microscopy and Vickers microhardness testing. The results showed that the shrouded titanium coatings exhibited an enhanced microstructure. The presence of the shroud and shroud gas flow led to a significant reduction in coating porosity because the reduction in air entrainment with the shroud resulted in better heating of the particles. The shrouded titanium coatings had a lower value of Vickers microhardness and a relative lower standard deviation than the air plasma sprayed titanium coatings

Mechanical and electrochemical properties of multiple-layer diode laser cladding of 316L stainless steel

In the present investigation, a detailed mechanical and electrochemical properties of multiple-layer laser clad 316L stainless steel (from the powders produced by gas atomized route) has been carried out. Multiple-layer laser cladding of 316L stainless steel has been conducted using a diode laser. The mechanical property (rmcrohardness) of the fabricated product has been evaluated using a microhardness testing machine and correlated with the process parameters. The electrochemical property, mainly pitting corrosion resistance of the fabricated layer corresponding to maximum microhardness (in a 3.56% NaCl solution) has been evaluated using standard potentiodynamic polarization testing. The microhardness of the laser assisted fabricated layers was found to vary from 170 to 278 VHN, increased with decrease in applied power density and increase in scan speed and was higher than that of conventionally processed 316L (155 VHN). The superior microhardness value is attributed to grain refinement associated with laser melting and rapid solidification. The critical potential to pit formation (E-PP1) was measured to be 550 mV saturated calomel electrode (SCE) and superior to the conventionally processed 316L stainless steel (445 mV (SCE)). (c) 2005 Elsevier B.V. All rights reserved

Surface microhardening studies on steels after high feed milling

The paper deals with the impact of high-speed machining production methods on the integrity of component surfaces. One has to point out that cutting conditions during machining have a significant impact on the final properties of surface and subsurface layers of the workpiece. The conclusion summarizes and analyzes the achieved results of experimental activities on stainless austenitic steel 1.4301, hardened tool steel 1.2343 and high-speed steel 1.3344 (ASP 2023). The results of the work experimental parts demonstrate the influence of cutting parameters on selected surface integrity ones, specifically strengthening the surface and subsurface layers. The performed experiments show that microhardness of a surface layer of the machined material can be influenced by suitable cutting conditions and other cutting process parameters.Web of Science12223022

Nano- and micromechanical properties of dentine: Investigation of differences with tooth side

NOTICE: this is the author’s version of a work that was accepted for publication in Journal of Biomechanics. Changes resulting from the publishing process, such as peer review, editing, corrections, structural formatting, and other quality control mechanisms may not be reflected in this document. Changes may have been made to this work since it was submitted for publication. A definitive version was subsequently published in Journal of Biomechanics, [VOL 44, (2011)] DOI: 10.1016/j.jbiomech.2011.03.00

Phase Composition and Defect Substructure of Strengthening Layer Surfaced on Low Alloyed Steel

The microstructure and microhardness distribution in surface of low carbon Hardox 450 steel coated with alloyed powder wires of different chemical compositions are studied. It is shown that the microhardness of 6-8 mm thickness surfaced layer exceeds that of base metal by more than 2 times. The increased mechanical properties of surfaced layer are caused by the submicro and nanoscale dispersed martensite, containing the niobium carbides Nb2C, NbC and iron borides Fe2B. In the bulk plates a dislocation substructure of the net-like type with scalar islocation density of 10^11 cm^-2 is observed. The layer surfaced with the wire containing B possesses the highest hardness. The possible mechanisms of niobium and boron carbides formation in surfacing are discusse

Mechanical property evaluation of an Al-2024 alloy subjected to HPT processing

An aluminum-copper alloy (Al-2024) was successfully subjected to high-pressure torsion (HPT) up to five turns at room temperature under an applied pressure of 6.0 GPa. The Al-2024 alloy is used as a fuselage structural material in the aerospace sector. Mechanical properties of the HPT-processed Al-2024 alloy were evaluated using the automated ball indentation technique. This test is based on multiple cycles of loading and unloading where a spherical indenter is used. After two and five turns of HPT, the Al-2024 alloy exhibited a UTS value of ~1014 MPa and ~1160 MPa respectively, at the edge of the samples. The microhardness was measured from edges to centers for all HPT samples. These results clearly demonstrate that processing by HPT gives a very significant increase in tensile properties and the microhardness values increase symmetrically from the centers to the edges. Following HPT, TEM examination of the five-turn HPT sample revealed the formation of high-angle grain boundaries and a large dislocation density with a reduced average grain size of ~80 nm. These results also demonstrate that high-pressure torsion is a processing tool for developing nanostructures in the Al-2024 alloy with enhanced mechanical propertie

Effect of processing condition and composition on the microhardness of Cu-(2.5-10)vol.%Al₂O₃ nanocomposite powder particles produced by high energy mechanical milling

Nanostructured Cu-(2.5-10vol.%)Al₂O₃ nanocomposites were produced using high energy mechanical milling. For the as-milled Cu- Al₂O₃ composite powder particles having Al₂O₃ volume fractions of 2.5% and 5%, the increase in average microhardness is significant with the increase of milling time from 12 hours to 24 hours. With the increase of the content of Al₂O₃ nanoparticles the microhardness increases and in the range of 255HV-270HV. The milled nanocomposite powders were heat treated at 150, 300, 400 and 500°C for 1 hour, respectively, to determine the thermal stability of the powder particles as a function of annealing temperature. The average microhardness increased/decreased for the Cu- Al₂O₃ composites after annealing at 150°C due to the dislocation density, while increasing the annealing temperature to 300°C and 400°C the average microhardness almost remained mostly unchanged. Further increasing the annealing temperature to 500°C causes significant decrease in average microhardness due to reduction in dislocation density and coarsening of Cu grains of the Cu- Al₂O₃ composite powders produced after 24 hours of milling. This paper is to report and discuss the changes of the microhardness of the material, caused by the compositions and processing conditions, used to fabricate the Cu-(2.5-10)vol.% Al₂O₃ nanocomposite powders

Single sided single pass submerged arc welding of austenitic stainless steel

The weld metal produced from a series of high productivity welds of 316LN austenitic stainless steel plate was examined to evaluate the effects of the use of a higher heat input process (> 2.5kJ/mm).This high heat input process was aimed at maximising single sided weld metal penetration in a single pass using simple square edge preparations and minimising time consuming handling operations. The evaluation was undertaken by correlating the local microstructure with the local toughness and microhardness of the cap, middle and root of the weld. It was established that the intermetallic phases / carbides present did not appear to have a significantly adverse effect on either corrosion or toughness. The phases observed and confirmed by the use of SAED were predominantly chi (χ) with some sigma( σ). No identifications were made of M23C6 which was observed in other studies of 316LN welds. A series of impact tests with variations in the notch positions showed that the thickness of the delta ferrite had an effect on the weld metal toughness. As a result of this work it was established that similar volume fractions of delta ferrite did not necessarily produce similar levels of weld metal toughness, but ferrite thickness did appear to have a contributory effect. Welding of 316LN stainless steel with a single sided single pass submerged arc welding process was satisfactorily undertaken up to 20mm plate thickness without preheat or post weld heat treatment. The ability to achieve this resulted in significant economic savings within the process for ship panel production combined with satisfactory weld metal properties